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51.
Qing-Song Yao Zhong-Chao Li Zai-Meng Qiu Fen Zhang Xiao-Bo Chen Dong-Chu Chen Shao-Kang Guan Rong-Chang Zeng 《稀有金属(英文版)》2019,(7)
Mg(OH)_2/Mg-Al-layered double hydroxide(LDH)coatings were modified with methyltrimethoxysilane(MTMS)on magnesium alloys.Effect of hydrolysis degree of silane solution on coating formation was investigated.Chemical compositions and surface morphologies of the coatings were examined using X-ray diffraction(XRD),Fourier transform infrared spectroscopy(FTIR),X-ray photoelectron spectroscopy(XPS)and field-emission scanning electronic microscopy(FESEM).Results indicated that the composite coatings consisted of polymethyltrimethoxysilane(PMTMS),LDH and Mg(OH)_2.Electrochemical and hydrogen evolution measurements revealed that the composite coatings possessed good corrosion resistance,especially the ones prepared in a high hydrolysis degree of silane.The optimum corrosion resistance of the composite coating was LDH/PMTMS-3 coating,which had the lowest value of corrosion current density(5.537 × 10~(-9) A·cm~(-2))and a dense surface.Plausible mechanism for coating formation and corrosion process of MTMS-modified Mg(OH)_2/Mg-Al-LDH coatings were discussed. 相似文献
52.
目的 为了提高扫地机器人的自主性和智能化程度,为扫地机器人配备视觉传感器,使其获得视觉感知能力,通过研究有效的垃圾检测分类模型与算法,实现对垃圾的定位与识别,引导扫地机器人对垃圾进行自动识别与按类处理,提高工作的目的性和效率,避免盲动和减少能耗。方法 选择检测速度较快的YOLOv2作为主网络模型,结合密集连接卷积网络,嵌入深层密集模块,对YOLOv2进行改进,提出一种YOLOv2-dense网络,该网络可以充分利用图像的高分辨率特征,实现图像浅层和深层特征的复用与融合。结果 测试结果表明,智能扫地机器人使用本文方法可以有效识别不同形态的常见垃圾类别,在真实场景中,测试识别准确率为84.98%,目标检测速度达到26帧/s。结论 实验结果表明,本文构建的YOLOv2-dense网络模型具有实时检测的速度,并且在处理具有不同背景、光照、视角与分辨率的图片时,表现出较强的适应和识别性能。在机器人移动过程中,可以保证以较高的准确率识别出垃圾的种类,整体性能优于原YOLOv2模型。 相似文献
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Polyimide microspheres were prepared via non‐aqueous emulsion polymerization by using pyromellitic dianhydride (PMDA) as anhydride monomer and 2,2‐bis(4‐(4‐aminophenoxy)phenyl)propane as amine monomer. The polyimide microspheres were well characterized by Fourier transform infrared spectroscopy, SEM and laser particle size analyzer. They were spherical in shape and monodisperse and their size was 31–33 μm. Polyimide mixtures formed by polyimide microspheres as fillers and polyimide composed of pyromellitic and dianhydride 4,4′‐oxydianiline (ODA) as matrix were investigated with regard to thermal properties, dielectric properties and mechanical properties. With 10%–50% polyimide microspheres in the polyimide mixtures, the dielectric constants were 2.26–2.48 (1 MHz) and the loss tangents were 0.00663–0.00857 (1 MHz), which were both significantly lower than the values for ODA‐PMDA polyimide. The decomposition temperature and glass transition temperature were above 440 and 290 °C. The polyimide mixtures possessed excellent thermal resistance. When the percentage of polyimide microsphere addition was 30%, the polyimide mixtures had the largest tensile strength (128.50 MPa) and elongation at break (9.01%). These results indicate that the polyimide microspheres were used as both low dielectric fillers and reinforcing fillers. © 2020 Society of Chemical Industry 相似文献
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Xiaoqiang Li Ting Cao Minai Zhang Hao Qiu Yang Huang Shengguan Qu Liang Liang Tao Song 《International Journal of Applied Ceramic Technology》2020,17(3):941-948
Porous fibers are widely used in catalysis chemistry and hydrogen storage but are rarely used in structural ceramics. In this study, spark plasma sintering was used to prepare an ultrafine porous boron nitride nanofiber-toughened WC composite for the first time. The obtained WC-0.05 wt% ultrafine porous boron nitride nanofiber composites exhibited better properties (ie, a 2.3% increase in hardness and a 19.6% increase in fracture toughness) compared to those of the pure WC specimen. The fiber porosity improved the second phase-WC matrix microstructural combination. The described approach is a novel preparation method for the WC composites. Furthermore, a new toughening mechanism, which is based on “pinning and stretching”, was determined. These findings suggest that porous boron nitride fibers can be considered to be second phases for toughening the WC composites. 相似文献
57.
In this paper, a triple shape memory material was prepared by ultra‐simple melt blending from poly(ε‐caprolactone) (PCL), poly(propylene carbonate) (PPC) and ethylene‐α‐octene block copolymer (OBC). The obtained material possessed a co‐continuous phase morphology and presented an excellent triple shape memory effect (triple‐SME). Theoretical prediction demonstrated that a special continuous phase morphology could be constructed by adjusting the proportions of the blend. Moreover, the results indicated that a close relationship existed between the phase morphology and the triple‐SME of PCL/PPC/OBC. The sample with 35 vol% PPC content contributed to the formation of a continuous phase morphology and exhibited the optimal triple‐SME. Additionally, the sample PCL/PPC/OBC (32.5/35/32.5) showed outstanding structure and performance stability during cycle loading–unloading tests, which evidenced the prominent cycling shape memory property (nearly 100% shape fixing and recovery of temporary shape). Overall, this work could provide an efficient, convenient and recyclable method to obtain high‐performance shape memory materials. © 2020 Society of Chemical Industry 相似文献
58.
为解决掘进成本较高、接替紧张等问题,基于1226工作面地质条件,对运输巷进行切顶卸压沿空留巷设计,主要包括切顶预裂缝、恒阻大变形锚索和巷道支护参数的设计,取得较好效果。 相似文献
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60.
Jialong Tian M. Babar Shahzad Wei Wang Lichang Yin Zhouhua Jiang Ke Yang 《材料科学技术学报》2018,34(9):1671-1675
The effect of Co addition on the formation of Ni-Ti clusters in maraging stainless steel was studied by three dimensional atom probe (3DAP) and first-principles calculation. The cluster analysis based on the maximum separation approach showed an increase in size but a decrease in density of Ni-Ti clusters with increasing the Co content. The first-principles calculation indicated weaker Co-Ni (Co-Ti) interactions than Co-Ti (Fe-Ti) interactions, which should be the essential reason for the change of distribution characteristics of Ni-Ti clusters in bcc Fe caused by Co addition. 相似文献